Description The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 is broken down into Section 1: a) Introduction; b) Dual bonding; c) The Element Nitrogen; d) The element oxygen; e) The element chlorine; f) Introduction to filtration; 1) Gravity filtration; a) Fluting Filter Paper for use in gravity filtration; 2) Vacuum Filtration (suction filtration); a) General Laboratory Techniques: Methods of heating; 1) Free flame; 2) Steam bath, or water bath; 3) Oil bath; 4) Electric Heating Mantles; 5) Hot Plates; a) Methods of Cooling; 1) Cold water bath; 2) Ice water bath; 3) Standard ice bath; 4) Salt/ice bath; 5) Dry ice/acetone bath; a) Cooling tricks of the trade; b) Recrystallization, and solid product recovery; c) Recrystallization; 1) General recrystallization utilizing heat only; a) Working example of recrystallization using heat only; 2) Recrystallization using seed crystals; 3) Recovering the product through low heat and vacuum; a) Washing liquids; b) Washing solids using non-vacuum techniques; c) Washing solids using vacuum techniques; d) Drying solids; e) Drying liquids to remove water; f) Laboratory safety; g) Laboratory glassware; h) Laboratory equipment
Section 2: Intermediates, Reagents, and Solvents
Section 3: Experimental Explosives Chemistry
Theoretical Preparation 1: 1,3,5-trinitrohexazinane
Azinane
Theoretical Preparation 2: trisodium hexazinane-1,3,5-triide
SOD
Theoretical Preparation 3: 3,3\',3\'\'-hexazinane-1,3,5-triyltris(triaza-1,2-dien-2-ium-1-ide)
HEXAAZIDE
HTA
Theoretical Preparation 4: diammonium trioxidane-1,3-diide; diammonium trioxide
DATD
Theoretical Preparation 5: 3,3\'-trioxidane-1,3-diylbis(triaza-1,2-dien-2-ium-1-ide)
TDTD
Theoretical Preparation 6: benzene-1,3,5-triyltris(chlorane) nonaoxide
BTCN
Chlorane
Theoretical Preparation 7: 2,4,6-trinitro-1,3,5,2,4,6-trioxatriazinane
TNTOTA; oxatriazinane
Theoretical Preparation 8: (2,4,6-trinitrobenzene-1,3,5-triyl)tris(chlorane) nonaoxide
Chlorane
Theoretical Preparation 9: 1,3,5-triazido-2,4,6-trinitrobenzene
Nitrazide
TATNB
Theoretical Preparation 10: 1,3,5-trinitrohexasilinane; nitrosilane; 2-TNHS
Theoretical Preparation 11: 1,3,5-trinitro-1,3,5-tris(nitrooxy)hexasilinane-1,3,5-triium
TNNHS
Si-135
Theoretical Preparation 12: 1,3,5-trinitrohexaphosphinane
TNHP
High Explosive Phosphorus
Theoretical Preparation 13: pentanitro-l5-phosphane; 5-PNP
Theoretical Preparation 14: trinitroamine oxide
TNAOX
NITROXIDE
Theoretical Preparation 15: pentachloryl-l5-phosphane
Theoretical Preparation 16: Tetranitrodiborane
TNDB
Nitro Boron
Theoretical Preparation 17: 1,2,3,4,5,6-hexanitrocyclohexaborane
KNCHB; 6-Nitrocycloborane
Theoretical Preparation 18: N\'-perchlorylperchloric hydrazide
N\'PCPH, Perchloryl hydrazine
Theoretical Preparation 19: tetranitrohydrazine
TNH-X
Theoretical Preparation 20: hexaaza-1,2,4,5-tetraene-2,5-diium-1,6-diide
Hexazide
HTDD
Theoretical Preparation 21: hexaazidobenzene
HAAB; 6-Azide
Theoretical Preparation 22: 1,2,3,4,5,6-hexanitro-1l4,2l4,3l4,4l4,5l4,6l4-hexathiine
Nitro hexathiine
Gamma-HNH
Theoretical Preparation 23: pentakis(dioxidobromanyl)-l5-chlorane
Chlorane; pentabromate chloride
PDDBC
Theoretical Preparation 24: hexa-1,3,5-triyne-1,6-diyl dinitrate
HTDD; poly acetylene dinitrate
Theoretical Preparation 25: 1,2,3,4,5,6-hexanitrohexa-1,3,5-triene-1,6-diyl dinitrate
HNHTDD
Hexanitro-Triene
Triene dinitrate
Theoretical Preparation 26: (1Z,3E,5Z)-1,2,3,4,5,6-hexaazidohexa-1,3,5-triene-1,6-diyl dinitrate
EZ-Azido Triene
HAHTDN
Theoretical Preparation 27: 1,2,3,4,5,6-hexafluoro-1,2,3,4,5,6-hexaperchlorylhexane-1,6-diyl dinitrate
Fluoroperchlorylhexane
HFGPHDD
Theoretical Preparation 28: 3,3\':4\',3\'\'-ter-1,2-dioxetane-4,4\'\'-diyl dinitrate
Dioxetane
Dioxetane dinitrate; ter-DDD
Theoretical Preparation 29: 2H,3\'H,3"H-2,2\':3\',2"-teraluminum-3,3"-diyl dinitrate
Aluminum-3H-dinitrate
Aluminum-3-3-dinitrate; 2H\'3H\'-Aluminum d.
Description The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 is broken down into Section 1: a) Introduction; b) Dual bonding; c) The Element Nitrogen; d) The element oxygen; e) The element chlorine; f) Introduction to filtration; 1) Gravity filtration; a) Fluting Filter Paper for use in gravity filtration; 2) Vacuum Filtration (suction filtration); a) General Laboratory Techniques: Methods of heating; 1) Free flame; 2) Steam bath, or water bath; 3) Oil bath; 4) Electric Heating Mantles; 5) Hot Plates; a) Methods of Cooling; 1) Cold water bath; 2) Ice water bath; 3) Standard ice bath; 4) Salt/ice bath; 5) Dry ice/acetone bath; a) Cooling tricks of the trade; b) Recrystallization, and solid product recovery; c) Recrystallization; 1) General recrystallization utilizing heat only; a) Working example of recrystallization using heat only; 2) Recrystallization using seed crystals; 3) Recovering the product through low heat and vacuum; a) Washing liquids; b) Washing solids using non-vacuum techniques; c) Washing solids using vacuum techniques; d) Drying solids; e) Drying liquids to remove water; f) Laboratory safety; g) Laboratory glassware; h) Laboratory equipment
Section 2: Intermediates, Reagents, and Solvents
Section 3: Experimental Explosives Chemistry
Theoretical Preparation 1: 1,3,5-trinitrohexazinane
Azinane
Theoretical Preparation 2: trisodium hexazinane-1,3,5-triide
SOD
Theoretical Preparation 3: 3,3\',3\'\'-hexazinane-1,3,5-triyltris(triaza-1,2-dien-2-ium-1-ide)
HEXAAZIDE
HTA
Theoretical Preparation 4: diammonium trioxidane-1,3-diide; diammonium trioxide
DATD
Theoretical Preparation 5: 3,3\'-trioxidane-1,3-diylbis(triaza-1,2-dien-2-ium-1-ide)
TDTD
Theoretical Preparation 6: benzene-1,3,5-triyltris(chlorane) nonaoxide
BTCN
Chlorane
Theoretical Preparation 7: 2,4,6-trinitro-1,3,5,2,4,6-trioxatriazinane
TNTOTA; oxatriazinane
Theoretical Preparation 8: (2,4,6-trinitrobenzene-1,3,5-triyl)tris(chlorane) nonaoxide
Chlorane
Theoretical Preparation 9: 1,3,5-triazido-2,4,6-trinitrobenzene
Nitrazide
TATNB
Theoretical Preparation 10: 1,3,5-trinitrohexasilinane; nitrosilane; 2-TNHS
Theoretical Preparation 11: 1,3,5-trinitro-1,3,5-tris(nitrooxy)hexasilinane-1,3,5-triium
TNNHS
Si-135
Theoretical Preparation 12: 1,3,5-trinitrohexaphosphinane
TNHP
High Explosive Phosphorus
Theoretical Preparation 13: pentanitro-l5-phosphane; 5-PNP
Theoretical Preparation 14: trinitroamine oxide
TNAOX
NITROXIDE
Theoretical Preparation 15: pentachloryl-l5-phosphane
Theoretical Preparation 16: Tetranitrodiborane
TNDB
Nitro Boron
Theoretical Preparation 17: 1,2,3,4,5,6-hexanitrocyclohexaborane
KNCHB; 6-Nitrocycloborane
Theoretical Preparation 18: N\'-perchlorylperchloric hydrazide
N\'PCPH, Perchloryl hydrazine
Theoretical Preparation 19: tetranitrohydrazine
TNH-X
Theoretical Preparation 20: hexaaza-1,2,4,5-tetraene-2,5-diium-1,6-diide
Hexazide
HTDD
Theoretical Preparation 21: hexaazidobenzene
HAAB; 6-Azide
Theoretical Preparation 22: 1,2,3,4,5,6-hexanitro-1l4,2l4,3l4,4l4,5l4,6l4-hexathiine
Nitro hexathiine
Gamma-HNH
Theoretical Preparation 23: pentakis(dioxidobromanyl)-l5-chlorane
Chlorane; pentabromate chloride
PDDBC
Theoretical Preparation 24: hexa-1,3,5-triyne-1,6-diyl dinitrate
HTDD; poly acetylene dinitrate
Theoretical Preparation 25: 1,2,3,4,5,6-hexanitrohexa-1,3,5-triene-1,6-diyl dinitrate
HNHTDD
Hexanitro-Triene
Triene dinitrate
Theoretical Preparation 26: (1Z,3E,5Z)-1,2,3,4,5,6-hexaazidohexa-1,3,5-triene-1,6-diyl dinitrate
EZ-Azido Triene
HAHTDN
Theoretical Preparation 27: 1,2,3,4,5,6-hexafluoro-1,2,3,4,5,6-hexaperchlorylhexane-1,6-diyl dinitrate
Fluoroperchlorylhexane
HFGPHDD
Theoretical Preparation 28: 3,3\':4\',3\'\'-ter-1,2-dioxetane-4,4\'\'-diyl dinitrate
Dioxetane
Dioxetane dinitrate; ter-DDD
Theoretical Preparation 29: 2H,3\'H,3"H-2,2\':3\',2"-teraluminum-3,3"-diyl dinitrate
Aluminum-3H-dinitrate
Aluminum-3-3-dinitrate; 2H\'3H\'-Aluminum d
